In Situ Hydrogen Loading on Zirconium Powder

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In Situ Hydrogen Loading on Zirconium Powder

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Publication Article, peer reviewed scientific
Title In Situ Hydrogen Loading on Zirconium Powder
Author(s) Maimaitiyili, Tuerdi ; Blomqvist, Jacob ; Steuwer, Axel ; Christina, Bjerkén ; Zanellato, Olivier ; Blackmur, Matthew ; Andrieux, Jerome ; Ribeiro, Fabienne
Date 2015
English abstract
For the first time, various hydride phases in a zirconium-hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were monitored in real time during hydrogenation and dehydrogenation, then whole pattern crystal structure analysis such as Rietveld and Pawley refinements were performed. All commonly reported low-pressure phases presented in the Zr-H phase diagram are obtained from a single experimental arrangement.
DOI (link to publisher's fulltext)
Publisher International Union of Crystallography
Host/Issue Journal of Synchrotron Radiation;4
Volume 22
ISSN 1600-5775
Pages 995-1000
Language eng (iso)
Subject(s) zirconium hydride
synchrotron X-ray diffraction
in situ hydrogen charging
hydrogen-induced degradation
phase transformation
Humanities/Social Sciences
Research Subject Categories::TECHNOLOGY
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