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  • 1.
    Maimaitiyili, Tuerdi
    et al.
    Malmö högskola, Faculty of Technology and Society (TS).
    Bjerkén, Christina
    Malmö högskola, Faculty of Technology and Society (TS).
    Steuwer, A.
    Wang, Z.
    Daniels, J.
    Andrieux, J.
    Blomqvist, Jakob
    Malmö högskola, Faculty of Technology and Society (TS).
    Zanellato, O.
    In situ observation of gamma-ZrH formation by X-ray diffraction2017In: Journal of Alloys and Compounds, ISSN 0925-8388, E-ISSN 1873-4669, Vol. 695, p. 3124-3130Article in journal (Refereed)
    Abstract [en]

    We report on the measurement of the formation of gamma-ZrH during in situ gaseous charging. The measurements were undertaken using high-energy synchrotron X-ray diffraction. Experimental observation shows that gamma-ZrH can form at 180 degrees C from a mixture of alpha+delta while dehydrogenating at slow cooling rates. The observation is further supported by ex situ laboratory X-ray diffraction on deuterated Zr powder that has undergone a similar heat-treatment cycle. The crystal structure of gamma-ZrH refinement agrees with the reported P4(2)/n structure found in the literature. (C) 2016 Elsevier B.V. All rights reserved.

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